Physical and chemical techniques have gained special interest for discovery of novel materials, nanoparticles characterization, crystals and metallic based characterization and semiconductor based materials. Nanotechnology has made tremendous advances and infinitely divisible into smaller pieces, or composed of small, indivisible and indestructible particles in the form atoms. Different approaches have used for designing of nanoparticles. Physical and chemical methods have been used for the synthesis of nanoparticles, although, some of them needed more advances for high quality and biodegradable materials to meet the industrial demands. Carbon and silica based nanoparticles can be designed in order to improve the rubber properties , while on the other hand, carbon based nanoparticles can be used for improving the polymers to increase their strength and impact resistance. Semiconductor quantum dots also made revolutionary advances for replacing the toxic materials employed. Nuclear magnetic resonance spectroscopy is the most important type of spectroscopy that helpful for industrial promotions of magnetic nanoparticles. High-performance liquid chromatography is the most important technique used in physics and chemistry in components in the given sample can be identifying easily within short period of time. Different nanoparticles can be easily accessed through Powder X-ray diffraction. One of the examples is silver nanoparticles. Crystallization is one of the most important process for solidification of atoms or molecules in such a way that they get shape the crystal.